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国家高技术研究发展计划(05H055)

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相关作者:郭栋杨跃罗娟田之悦成丽更多>>
相关机构:四川大学更多>>
发文基金:国家高技术研究发展计划更多>>
相关领域:理学更多>>

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微波辐射在合成沙利度胺的铵盐类衍生物中的应用
2009年
Amino acid benzyl ester p-toluenesulfonic acids were synthesized under microwave irradiation condition by reaction of four amino acids with benzyl alcohol and p-toluenesulfonic acid,and then reacted with the N-phthaloyl-L-glutamic anhydride to yield compound 3a-d,hydrogenised and treated with NH3(g) to obtain the target compounds—thalidomide ammonium salt derivatives.The microwave-assisted method was used to synthesis the thalidomide amino acid benzyl ester p-tolunensulfonic acid,the reaction time was brought down with improved yield as compared with conventional heating method.The structures were comfirmed by MS,1H-NMR and elemental analysis.
郭举郑永胜郭栋汪宏于姝燕杨跃田之悦罗娟成丽
关键词:微波辐射
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