Super-high pressure(SHP)technique plays an increasing role in the fields of materials science and engineering.Herein,the Mg_(97)Zn_(1)Y_(2) alloy was heat-treated under SHP(6 GPa)by cubic-anvil large-volume press with six rams for 2 h in the temperature range of 500–1200℃.The microstructure and mechanical properties were investigated.The results indicated that the as-cast sample consists of α-Mg equiaxed dendrites and continuous lamellar long period stacking ordered(LPSO)phase in grain boundaries.After the SHP treatment,the LPSO phase is gradually replaced by eutectic phase(Mg,Zn)_(3)Y with increasing temperature.The microhardness and strength of sample prepared at 1100℃ under SHP treatment are significantly improved compared with the as-cast one at room temperature.The improved mechanical behaviors are mainly attributed to LPSO phase kink-banding strengthening at low temperature and the precipitation strengthening of a large amount of fine(Mg,Zn)_(3)Y particles at high temperature after SHP treatment.It reveals the SHP is an effective approach to prepare high performance Mg alloys.