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国家自然科学基金(11232008)

作品数:20 被引量:66H指数:5
相关作者:谢惠民刘战伟郭小钧汪长安朱建国更多>>
相关机构:清华大学北京理工大学江苏大学更多>>
发文基金:国家自然科学基金国家重点基础研究发展计划清华大学自主科研计划更多>>
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20 条 记 录,以下是 1-10
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La_2Zr_2O_7空心陶瓷粉体的制备被引量:1
2015年
本研究使用胶体碳球为硬模板,合成制备得到La_2Zr_2O_7壳层结构材料。通过X-ray衍射仪、红外光谱仪、扫描电子显微镜(SEM)、透射电子显微镜(TEM)等分析技术对材料的物相结构、表面基团、显微结构等进行表征;研究碱处理对胶体碳球表面荷电性质的影响,La^(3+)和Zr^(4+)包裹时的最佳离子浓度比。结果表明,水热法制备胶体碳球的实验条件为:浓度0.3 mol/L、时间8 h、温度190℃;碱处理碳球的最佳条件:5 mol/L Na OH溶液中处理12 h;金属离子La^(3+)和Zr^(4+)包裹碳球的最佳摩尔质量比m(La^(3+)):m(Zr^(4+))=2:1。所得La2Zr2O7空心微球的直径为230 nm,球壳厚度为10~15 nm。
赵禹程郭小钧李洒汪长安
关键词:热障涂层LA2ZR2O7
Coherent gradient sensing method for measuring thermal stress field of thermal barrier coating structures
2017年
Coherent gradient sensing(CGS)method can be used to measure the slope of a reflective surface,and has the merits of full-field,non-contact,and real-time measurement.In this study,the thermal stress field of thermal barrier coating(TBC)structures is measured by CGS method.Two kinds of powders were sprayed onto Ni-based alloy using a plasma spraying method to obtain two groups of film–substrate specimens.The specimens were then heated with an oxy-acetylene flame.The resulting thermal mismatch between the film and substrate led to out-of-plane deformation of the specimen.The deformation was measured by the reflective CGS method and the thermal stress field of the structure was obtained through calibration with the help of finite element analysis.Both the experiment and numerical results showed that the thermal stress field of TBC structures can be successfully measured by CGS method.
Kang MaHuimin Xie
Characterization for elastic constants of fused deposition modelling-fabricated materials based on the virtual fields method and digital image correlation被引量:3
2017年
Fused deposition modelling(FDM), a widely used rapid prototyping process, is a promising technique in manufacturing engineering. In this work, a method for characterizing elastic constants of FDM-fabricated materials is proposed. First of all, according to the manufacturing process of FDM, orthotropic constitutive model is used to describe the mechanical behavior. Then the virtual fields method(VFM) is applied to characterize all the mechanical parameters(Q_(11), Q_(22), Q_(12), Q_(66)) using the full-field strain,which is measured by digital image correlation(DIC). Since the principal axis of the FDM-fabricated structure is sometimes unknown due to the complexity of the manufacturing process, a disk in diametrical compression is used as the load configuration so that the loading angle can be changed conveniently. To verify the feasibility of the proposed method, finite element method(FEM) simulation is conducted to obtain the strain field of the disk. The simulation results show that higher accuracy can be achieved when the loading angle is close to 30?. Finally, a disk fabricated by FDM was used for the experiment. By rotating the disk, several tests with different loading angles were conducted. To determine the position of the principal axis in each test, two groups of parameters(Q_(11), Q_(22), Q_(12), Q_(66)) are calculated by two different groups of virtual fields. Then the corresponding loading angle can be determined by minimizing the deviation between two groups of the parameters. After that, the four constants(Q_(11), Q_(22), Q_(12), Q_(66)) were determined from the test with an angle of 27?.
Quankun CaoHuimin Xie
关键词:FUSEDDEPOSITIONFIELDSORTHOTROPICCONSTITUTIVEDISK
聚合物膜上的微尺度金属导线在力电耦合作用下的屈曲行为(英文)被引量:2
2014年
研究一种典型的微尺度康铜线/聚合物膜结构在力电耦合作用下的屈曲行为。根据卸载后康铜线从聚合物基底上屈曲的现象,评估康铜线与聚合物基底间的界面韧性。此外,力电耦合作用还会诱发新的失稳模态。在电载荷和拉伸载荷作用下,康铜线易在屈曲时发生断裂。在电载荷和压缩载荷作用下,康铜线易在屈曲区域的顶部发生折叠,偶尔还会向聚合物基底内部方向发生屈曲。分析了这些失稳模态的产生机理。
王庆华岸本哲谢惠民李艳杰吴丹
关键词:失稳模态
热障涂层TEM原位加热下应力/应变演化的实验研究
热障涂层(TBCs)材料被广泛应用在航空发动机、涡轮机、汽轮机叶片等热端部件上,其高温失效问题是热障涂层材料研究的重要命题。本文结合高分辨透射电子显微镜(TEM)从纳观尺度研究了TBCs在高温服役情况下的应力/应变演化。...
张宏业温辉辉刘战伟谢惠民
关键词:TEM应力
Microstructural and mechanical properties of thermal barrier coating at 1400℃ treatment被引量:1
2014年
The mechanical properties of plasma-sprayed thermal barrier coating(TBC) play a vital role in governing their lifetime and performance. This work investigated the microstructural and mechanical properties of TBC with high temperature treatment at 1 400℃ by scanning electron microscopy and indentation.We calculated elastic modulus and hardness through the application of Weibull statistics analysis. The results indicate that the microstructure of ceramic coating will change continuously at high temperature, and accordingly the porosity decreases due to the grain growths and crack closes. In addition, the elastic modulus and hardness nonlinearly go up with the heat treatment time and go down with increasing porosity. This demonstrates that the microstructural evolution and porosity of TBC are caused by high temperature treatment, and as a result its mechanical properties are influenced.
Jianguo ZhuKang Ma
关键词:热障涂层扫描电子显微镜弹性模量
Residual stress evolution regularity in thermal barrier coatings under thermal shock loading被引量:4
2014年
Residual stress evolution regularity in thermal barrier ceramic coatings(TBCs) under different cycles of thermal shock loading of 1 100℃ was investigated by the microscopic digital image correlation(DIC) and micro-Raman spectroscopy, respectively. The obtained results showed that, as the cycle number of the thermal shock loading increases, the evolution of the residual stress undergoes three distinct stages: a sharp increase, a gradual change, and a reduction.The extension stress near the TBC surface is fast transformed to compressive one through just one thermal cycle. After different thermal shock cycles with peak temperature of 1 100℃, phase transformation in TBC does not happen, whereas the generation, development, evolution of the thermally grown oxide(TGO) layer and micro-cracks are the main reasons causing the evolution regularity of the residual stress.
Ximin ChenZhanwei LiuYang Yang
关键词:热障涂层冲击载荷作用拉曼光谱学
Elastic constants characterization on graphite at 500℃ by the virtual fields method被引量:1
2014年
In this paper the elastic constants of graphite at elevated temperature were experimentally investigated by using the virtual fields method(VFM). A new method was presented for the characterization of mechanical properties at elevated temperature. The three-point bending tests were performed on graphite materials by an universal testing machine equipped with heating furnace. Based on the heterogeneous deformation fields measured by the digital image correlation(DIC) technique, the elastic constants were then extracted by using VFM.The measurement results of the elastic constants at 500℃ were obtained. The effect on the experimental results was also analyzed. The successful results verify the feasibility of using the proposed method to measure the properties of graphite at high temperature, and the proposed method is believed to have a good potential for further applications.
Baoqiao GuoHuaixi WangHuimin XiePengwan Chen
关键词:石墨材料字段三点弯曲试验数字图像相关
曲面热障涂层中脱粘缺陷的精确定位
热障涂层(thermal barrier coatings,TBC)中脱粘缺陷的存在和演化是造成涡轮发动机叶片过早失效的关键问题之一。本文发展了针对复杂曲面构件缺陷检测的线激光热成像技术,利用线激光能够快速激发出TBC构...
焦大成; 石文雄; 刘战伟; 谢惠民;
关键词:热障涂层
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Identification of the elastic stiffness of composites using the virtual fields method and digital image correlation被引量:5
2015年
This paper presents an effective methodology for characterizing the mechanical parameters of composites using digital image correlation combined with the virtual fields method.By using a three-point bending test configuration,this method can identify all mechanical parameters of the material with merely a single test.Successful results verified that this method is especially effective for characterizing composite materials.In this study,the method is applied to measure the orthotropic elastic parameters of fiber-reinforced polymer-matrix composites before and after the hygrothermal aging process.The results indicate that the hygrothermal aging environment significantly influences the mechanical property of a composite.The components of the parameters in the direction of the fiber bundle decreased significantly.From the accuracy analysis,we found that the actual measurement accuracy is sensitive to a shift of the horizontal edges and rotation of the vertical edges.
Lebin JiangBaoqiao GuoHuimin Xie
关键词:纤维增强聚合物基复合材料数字图像相关弹性刚度湿热老化
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