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中国博士后科学基金(20110491492)

作品数:7 被引量:16H指数:2
相关作者:胡小武艾凡荣闫洪李双明蒋福刚更多>>
相关机构:南昌大学西北工业大学更多>>
发文基金:中国博士后科学基金国家自然科学基金江西省教育厅科学技术研究项目更多>>
相关领域:金属学及工艺一般工业技术化学工程更多>>

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7 条 记 录,以下是 1-7
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Sn基无铅钎料与Cu基板间化合物Cu_6Sn_5的研究进展被引量:5
2012年
主要介绍了Sn基无铅钎料和Cu基板在界面处反应生成的金属间化合物Cu6Sn5与焊接点可靠性的关系。综述了近年来Cu6Sn5的研究进展,内容包括:Sn基无铅钎料在Cu基板上形成的Cu6Sn5的生长形态、晶体取向、生长动力学以及纳米颗粒对界面Cu6Sn5尺寸及形貌的影响。
胡小武艾凡荣闫洪
Pb-Bi-Sn准包晶合金定向凝固微观组织演化
2012年
采用液态金属冷却定向凝固结合液淬法,在温度梯度为18K/mm、凝固速度为0.5~100μm/s的条件下系统研究了Pb-30%Bi-18%Sn准包晶合金的微观组织演化及溶质分布规律。主要从凝固路径、相组成、溶质分布及微观组织特征等几个方面来研究Pb-Bi—sn准包晶合金定向凝固过程的组织演化。其中,准包晶合金的凝固路径通过DSC差热分析的方法进行研究,发现其凝固路径为:L→L+α-Pb→L+α-Pb+β-PbTBi3→L+α-Pb+β-PbTBi3+Sn→(β-Pb7Bi+Sn)共晶。结合XRD,分析定向凝固试样的相结构,结果表明:试样由具有面心立方结构的α-Pb相、密排六方结构的β-Pb7Bi3相和体心正方结构的(Sn)相构成。在Pb-Bi-Sn合金定向凝固过程中,当凝固速度为0.5~2μm/s时,初生α-Pb相以胞状界面生长,而当凝固速度增大至5μm/s及以上时,初生α—Pb相将由胞状转变为枝晶状界面生长。利用能谱分析仪对定向凝固试样进行溶质分布测试,发现局部出现溶质偏析,导致共晶组织(β-PbTBi3+Sn)出现。
胡小武李双明艾凡荣蒋福刚
关键词:定向凝固溶质分布
Effect of sample diameter on primary and secondary dendrite arm spacings during directional solidification of Pb-26wt.%Bi hypo-peritectic alloy被引量:2
2011年
The microstructure scales of dendrites, such as primary and secondary dendrite arm spacings, control the segregation profiles and the formation of secondary phases within interdendritic regions, which determine the properties of solidified structures. Investigations on primary and secondary dendrite arm spacings of primary a-phase during directionally solidified Pb-26wt%Bi hypo-peritectic alloy were carried out in this research, and systematic studies were conducted using cylindrical samples with different diameters (Ф = 1.8 and 7.0 mm) in order to analyze the effects of sample diameter on the primary and secondary dendrite arm spacings. In this work, the dependence of dendrite arm spacings on growth velocity was established. In addition, the experimental data concerning the primary and secondary dendrite ann spacings were compared with the main predictive dendritic models from the literatures. A comparison between experimental results for dendrite arm spacings of the 1.8-mm-diameter sample and 7.0-ram-diameter sample was also conducted.
HU XiaowuYAN HongCHEN WenjingLI ShuangmingFU Hengzhi
关键词:DENDRITES
Pb-Bi包晶合金定向凝固过程中带状组织的形成(英文)被引量:1
2012年
采用Bridgman定向凝固技术对Pb-Bi包晶合金进行定向凝固实验,生长速度为0.5μm/s,温度梯度为35K/mm。在亚包晶和过包晶成分的Pb-Bi合金中(Pb-xBi,x=26%,28%,30%和 34%)均观察到带状组织。由于熔体对流的影响,在试样中心形成树状初生α相,周围被包晶β相基体包围。带状组织出现在树状组织后,并且该带状组织为过渡性的。测定带状组织中的成分分布,从而确定α和β两相的形核过冷度。在有限长试样中,熔体对流是形成过渡性带状组织的主要原因,该过渡性带状组织表现为有限带数,带宽不恒定,且在Pb-Bi合金的两相包晶区很宽的成分范围内出现。
胡小武李双明艾凡荣闫洪
关键词:定向凝固偏析
Pb-Bi包晶合金定向凝固相和组织选择
2012年
针对Pb-Bi包晶合金中高速及低速定向凝固,利用最高界面生长温度判据以及充分形核和成分过冷准则,对Pb-Bi包晶合金定向凝固中初生α和包晶β两相的相互竞争规律进行预测。计算结果表明:在中高速凝固段,与Pb-26%Bi、Pb-28%Bi、Pb-30%Bi和Pb-34%Bi(质量分数)合金对应的α→β转变的临界生长速度分别为20、14、8.5和2 mm/s;在低速凝固段,合金的相选择图分为8个生长区,其中包括两相分别以单相生长区及两相混合生长区。利用该相选择图,结合温度梯度与凝固速度比值(G/V)及合金原始成分(C0)可预测相选择规律及组织形态。
胡小武闫洪陈文静李双明傅恒志
关键词:包晶合金定向凝固相选择
Influences of pouring temperature and cooling rate on microstructure and mechanical properties of casting Al-Si-Cu aluminum alloy被引量:7
2012年
This paper investigated the influences of pouring temperature and cooling rate on the microstructure development and mechanical properties for casting A1-Si-Cu aluminum alloy. The microstructure of the as-cast samples was characterized by an optical microscope. The results showed that the dendrite arm spacing (DAS,),) is well refined by pouring at a higher temperature. The A decreases with increasing pouring temperature due to the multiplication of the nucleation sites in the superheating liquid melt, and the mechanical properties, such as microhardness and ultimate tensile strength increase correspondingly, while the elongation decreases. The relationships between microhardness and 3, for the samples cooled in metal mould and sand mould, are given as HV:l18.9 - 1.246A and HV=l15.2- 1.029A, respectively. The effects of the cooling rate controlled by using permanent mould casting and sand mould casing processes (the cooling medium is air and sand, respectively) on the dendrite arm spacing and mechanical properties are similar to the effect of the pouring temperature.
Xiaowu HUFanrong AIHong YAN
Research on lamellar structure and micro-hardness of directionally solidified Sn-58Bi eutectic alloy被引量:1
2012年
In this work,the Sn-58Bi(weight percent) eutectic alloy was directionally solidified at a constant temperature gradient(G = 12 K.mm-1) with different growth rates using a Bridgman type directional solidification furnace.A lamellar microstructure was observed in the Sn-58Bi samples.The lamellar spacing and micro-hardness of longitudinal and transversal sections were measured.The values of lamellar spacing of both longitudinal and transversal sections decrease with an increase in growth rate.The microhardness increases with an increase in the growth rate and decreases with an increase in the lamellar spacing.The dependence of lamellar spacing on growth rate,and micro-hardness on both growth rate and lamellar spacing were obtained by linear regression analysis.The relationships between the lamellar spacing and growth rate,microhardness and growth rate,and micro-hardness and lamellar spacing for transversal and longitudinal sections of Sn-58Bi eutectic alloy were given.The fitted exponent values obtained in this work were compared with the previous similar experimental results and a good agreement was obtained.
Hu XiaowuLi KeAi Fanrong
关键词:金属材料锡合金
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