The influence of chemical composition and cold deformation on aging precipitation behavior of 18Cr-16Mn-2Mo-1.1N(HNS-A), 18Cr-16Mn-1.3N(HNS-B), 18Cr-18Mn-2Mo-0.96N(HNS-C) and 18Cr-18Mn-2Mo-0.77N(HNS-D) high nitrogen austenitic stainless steels was investigated. The results show that the "nose" temperatures and incubation periods of the initial time temperature precipitation(TTP) curves of aged HNSs are found to be 850℃,60s; 850℃, 45s; 850℃, 60 s and 900℃,90s, respectively. Based on the analysis of SAD patterns, the coarse cellular Cr2N precipitate which presents a lamellar structure has a hexagonal structure of a=0.478 nm and c=0.444 nm. The χ phase corresponding to a composition of Fe36Cr12Mo10, is determined to be a body-centered cubic structure of a=0.892 nm. The precipitating sensitivity presents no more difference with the nitrogen content increasing from 0.77% to 0.96%, but exhibits so obviously that the cellular precipitates nearly overspread the whole field. The addition of Mo element can restrain the TTP curves moving left and down, which means decreasing the sensitivity of aging precipitation. With increasing the cold deformation, the sensitivity of precipitation increases obviously.
利用Gleeble-1500热模拟实验机进行压缩实验,研究了KT5331钢变形温度为850~1200℃,应变速率为0.01~12 s-1条件下的热变形行为。结果表明,随变形温度升高、应变速率降低,动态再结晶越容易发生,再结晶晶粒尺寸增加,完全动态再结晶温度约为1100℃。完全动态再结晶温度以下,随变形温度升高和应变速率降低,动态再结晶晶粒体积分数增加;完全动态再结晶温度以上,在低应变速率下,经60%压缩变形后,出现混晶形貌,应变速率较高时为等轴晶。通过拟合得到热变形激活能Q为436.541 k J/mol,建立了热变形双曲正弦本构方程,εexp（436541/RT）=6.12×101 5[sinh（0.009344σp）]4.739,具有较高预测精度,根据模型计算所得预测值与实验值之间的平均相对误差为5.9%。
