The complex(C24H24NO)2Cu·CH3CN（HL=S-（1-Benzy1-pyrrolidin-2-yl）-diphenyl-methanol）was （synthesized） by the electrochemical oxidation of Cu metal anodes in acetonitrile solution.The final product was （characterized） by elementary analysis,IR,and SEM and the structure was determined by single-crystal X-ray diffraction.The crystal belongs to trigonal,space group P3121 with a=9.8201（15）,b=9.82501（15）,c=36.516（6）?,α=β=90°,γ=120°,V=3049.6（8）?3,Z=3,ρcalc.=1.290g/cm3,F（000）=1251.In the complex two hydroxy oxygen atoms and two pyrrolidin nitrogen atoms from the ligand coordinate to copper（II）ion,forming a distorted square plane.
Microwave irradiation can accelerate the rate of the synthesis reaction of ferrocenyl α,β unsaturated ketones by using KF Al 2O 3 as a catalyst. Six fitled compounds were prepared with microware assisted synthesis. Their structures were characterized by 1H NMR, IR, and elemental analysis.
